Les nanoparticules de CuO_O2 sont lavées à partir d'acétone anhydre en boîte à gants. La poudre est séchée, pesée puis analysée en IR en mode ATR. Après lavage, les nanoparticules de CuO_air et de CuO_O2 perdent respectivement environ 72 et 87 % de leurs masses initiales. Les nanoparticules lavées sont diluées dans un volume de toluène connu et séparées en plusieurs échantillons, trois lavages à l'acétone sont effectués (centrifugation 10000 Tr.min -1 , 10 minutes) ,
, Afin d'avoir une surface oxydée, les substrats sont traités dans une solution Piranha (H2SO4 2 : H2O2 1), plongés dans un bain d'eau à 80 °C pendant 30 min. Les substrats sont ensuite séchés puis analysés en IR en mode transmission, en boîte à gants. L'alumine est ensuite déposée par ALD en salle blanche, utilisant 20 cycles de TMA et H2O. L'épaisseur (? 6 nm) est mesurée par un ellipsomètre. Les surfaces d'alumines sont lavées avant de les utiliser, Des substrats de Si (100) sont rincés respectivement dans du dichlorométhane, acétone et méthanol pendant 10 min dans un bain ultrasons
, Les nanoparticules des échantillons à l'état liquide (non lavées) sont déposées brut sur les surfaces de SiO2 avec un cycle de 1500 Tr.min -1 pendant 1 min. Les nanoparticules à l'état solide sont diluées dans du toluène sec pour avoir une solution de 5 mg.mL -1 , et déposées avec un cycle de 3000 Tr, Les nanoparticules sont déposées par spin-coating, en boîte à gants, sur les surfaces de SiO2 ou Al2O3
, Une solution de 1 mM d'acide 12-mercaptododecylphosphonique est préparée dans 18 mL de toluène. La surface d'alumine est immergée dans la solution pendant 1 nuit, à l'abri de la lumière. La surface est ensuite rincée au toluène pendant 10 min dans un bain à ultrasons
, Un deuxième volume d'hexane de 5 mL est versé pour nettoyer les bords du pilulier. Le pilulier contenant le mélange est placé dans un bécher rempli d'eau, et le tout est disposé dans un bain à ultrasons pendant 10 min. Le mélange est ensuite laissé reposer durant 1 jour pour permettre aux nanoparticules de sédimenter dans le fond du pilulier. Le prélèvement se fait à partir d, Suivant la stoechiométrie ? désirée, les poudres d'Al et de CuO sont pesées séparément puis introduites dans un pilulier contenant 5 mL d'hexane
, 29 mmol) et mélangées à l'OA (18,3 mg, 0,14 mmol) durant 1 heure. Le mélange est centrifugé (8700 Tr.min -1 , 10 minutes) and les nanoparticules de CuO_com@OA sont récupérées et séchées avant caractérisation et utilisation, Les nanoparticules de CuO_com sont pesées (500 mg, vol.6
, 04 mol) de THF en boîte à gants. La solution incolore est laissée pendant une durée de 30 minutes et le pilulier contenant la solution est placé dans un réacteur fermé, 365 mmol) de CuAmd sont dilués dans 3 mL
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